hiv注射治疗的稳定性指示方法stability indicating method for hiv injection treatment
conditions
column: ace excel 2 c18
dimensions: 50 x 3.0 mm
part number: exl -101-0503u
mobile phase:
a: 0.1% tfa in h2o
b: 0.1% tfa in mecn
gradient:
time(mins)
%b
0.0
10
3.0
90
6.0
90
6.1
10
8.0
10
flow rate: 0.4 ml/min
injection: 20 μl
temperature: 30 °c
detection: uv, 240 nm
analytes
1. emtricitabine(lloq 0.10 μg/ml)
2. tenofovir disoproxil(lloq 0.10 μg/ml)
3. cobicistat(lloq 0.20 μg/ml)
4. elvitegravir(lloq 0.02 μg/ml)
