口服液合成大麻素色谱分析synthetic cannabinoids (spice) from oral fluid
conditions
column: ace excel 2 c18-ar
dimensions: 100 x 2.1 mm
part number: exl -109-1002u
mobile phase: 0.1% formic acid in meoh/h2o (85:15 v/v)
flow rate: 0.3 ml/min
temperature: ambient
detection: applied biosystems/mds sciex 4000 q-trap positive mode turbo ionspray
extracted ion chromatogram for spice analytes fortified in neat oral fluid at 20 ng/ml